不同板材的除膠量測(cè)試報(bào)告

不同板材的除膠量實(shí)驗(yàn)報(bào)告一、 實(shí)驗(yàn)?zāi)康墓灸壳笆褂玫陌宀亩喾N多樣，沉銅前部分板材除膠流程無(wú)明確指示，通過(guò)本次實(shí)驗(yàn)評(píng)估確定不同板材的除膠流程。二、 測(cè)試流程測(cè)試片一烘板一冷卻一稱重一除膠一烘板一冷卻一稱重一計(jì)算除膠速率三、 測(cè)試片規(guī)格板材，①常用板材：S1170、S1141、S1000、IT180、IT158、IT140；②其它板材，S1180、S1165、S1155、S1000-2。測(cè)試片規(guī)格，尺寸15X10cm，板厚1.2—1.6mm。各種板材特性板材S1180S1170S1165S1155S1141S1000S1000-2IT180IT158IT140生益料，生益料，生益無(wú)生益無(wú)生益料，生益料，生益料，聯(lián)茂聯(lián)茂聯(lián)茂料，高TG，高TG，鹵素料，鹵素料，普通TG，中TG，中TG，料，中料，中普通TG，特性TG值TG值TG值TG值TG值TG值TG值TG，TGTG，TGTG值180°C，170C，170C，145C，135C，170C，150C，值180值150135C。無(wú)填料無(wú)填料。有填料。有填料。無(wú)填料。有填料有填料CC。四、測(cè)試項(xiàng)目相同除膠流程不同板材的除膠速率;相同板材不同除膠流程的除膠速率。五、實(shí)驗(yàn)結(jié)果水平沉銅線除膠流程⑴.水平除膠一次，速度1.0m/min。①.藥水狀態(tài)及處理時(shí)間缸位藥水濃度溫度/C處理時(shí)間/sec溶脹211：109%NaOH:0.96N83116除膠渣Namno4:56g/l；Na2mno4：16g/l；213B:1.26N86.7150

中和216—5：108.9%45.787中和 中和216—5：108.9%45.787②.除膠速率板材TG值/C。板厚/mm測(cè)試片序號(hào)測(cè)前稱重/g測(cè)后稱重/g除膠速率/mg/cm2平均值S11701701.3±0.1133.940933.92810.0430.038233.948533.93830.034S11651701.6±0.1341.849541.69890.5020.504442.056141.90420.506S11551451.1±0.1529.442129.39300.1640.152629.933429.89080.142S11411351.2±0.1732.993132.95910.1130.114833.062133.02790.114IT1581501.2±0.1932.578632.56420.0480.0521033.224933.20790.057IT1401351.3±0.11134.840634.75980.2690.2581234.522534.44880.246(2).水平除膠兩次，速度1.5m/min+1.0m/min。①.藥水狀態(tài)及處理時(shí)間缸位藥水濃度溫度/C處理時(shí)間/sec溶脹211：109%NaOH:0.96N83116+58除膠渣Namno4:56g/l；Na2mno4：16g/l；213B:1.26N86.7150+75中和216—5：108.9%45.787+43.5②.除膠速率板材TG值/C。板厚/mm測(cè)試片序號(hào)測(cè)前稱重/g測(cè)后稱重/g除膠速率/mg/cm2平均值S11801801.6±0.1143.569543.54430.0840.09242.878242.84950.096S11701701.3±0.1333.694533.67310.0710.0718433.970133.94840.072S11651701.6±0.1540.826640.55710.8980.941641.146540.85170.983S11551451.1±0.1729.668929.59730.2390.237830.110330.03960.236

S11411351.2±0.1932.823532.77720.1540.1551033.086133.03950.155S10001701.6±0.11144.606844.58640.0680.0691243.990843.96990.070S1000-21501.2±0.11332.398632.37070.0930.0951431.861731.83260.097IT1801801.4±0.11542.663542.64790.0520.0551642.213642.19620.058IT1581501.2±0.11733.229933.21020.0660.0641832.710732.69190.063IT1401351.3±0.11934.452634.31780.4490.4422034.763334.63270.435(3).水平除膠兩次，速度1.0m/min+1.0m/min。①.藥水狀態(tài)及處理時(shí)間缸位藥水濃度溫度/°c處理時(shí)間/sec溶脹211：109%NaOH:0.96N83116+116除膠渣Namno4:56g/l；Na2mno4:16g/l；213B:1.26N86.7150+150中和216—5：108.9%45.787+87②.除膠速率板材TG值/C。板厚/mm測(cè)試片序號(hào)測(cè)前稱重/g測(cè)后稱重/g除膠速率/mg/cm2平均值S11801801.6±0.1142.930242.89930.1030.112243.624543.58830.121S11701701.3±0.1334.048634.02370.0830.0815434.077134.05310.080S11651701.6±0.1542.010241.67781.1081.116642.255041.91761.125S11551451.1±0.1729.568929.48150.2910.291829.597329.51030.290S11411351.3±0.1933.027732.97930.1610.1641033.017132.96690.167S10001701.6±0.11144.211244.18370.0920.092

1244.870844.84310.092S1000-21501.2±0.11332.470632.43470.1200.1241432.119132.08070.128IT1801801.4±0.11542.781942.75760.0810.0851642.551142.52440.089IT1581501.2±0.11732.847232.81780.0980.0901832.925132.90010.083IT1401351.3±0.11934.730434.57490.5180.5332034.510134.34590.547⑷.垂直除膠+水平除膠，垂直除膠（溶脹8分鐘）,水平除膠速度速度1.0m/min。①.藥水狀態(tài)及處理時(shí)間工序缸位藥水濃度溫度/°c處理時(shí)間/sec水平除膠溶脹211：109%NaOH:0.96N84.2116除膠渣Namno4:56g/l；Na2mno4:16g/l；213B:1.26N87.4150中和216—5：108.9%45.187垂直除膠溶脹SW-110：33.8%70480除膠渣Kmno4:64.5g/l；K2mno4:28.6g/lNaOH:46.2g/l79390中和NU-121：2.13N40300除膠速率板材TG值/C。板厚/mm測(cè)試片序號(hào)測(cè)前稱重/g測(cè)后稱重/g除膠速率/mg/cm2平均值S11801801.6+0.1142.765342.70240.2100.193243.725943.67310.176S11651701.6+0.1341.942341.54551.3231.363441.651241.23051.402S10001701.6+0.1544.629344.58130.1600.161644.618944.57070.161S1000-21501.2+0.1732.050131.98430.2190.218

831.837131.77190.217IT1801801.4±0.1942.351742.30250.1640.1751042.598642.54310.185⑸.垂直除膠+水平除膠，垂直除膠（溶脹12分鐘），水平除膠速度速度1.0m/min。①.藥水狀態(tài)及處理時(shí)間工序缸位藥水濃度溫度/°c處理時(shí)間/sec水平除膠溶脹211：109%NaOH:0.96N84.2116除膠渣Namno4:56g/l；Na2mno4：16g/l；213B:1.26N87.4150中和216—5：108.9%45.187垂直除膠溶脹SW-110：33.8%70720除膠渣Kmno4:64.5g/l；K2mno4:28.6g/lNaOH:46.2g/l79390中和NU-121：2.13N40300②.除膠速率板材TG值/C。板厚/mm測(cè)試片序號(hào)測(cè)前稱重/g測(cè)后稱重/g除膠速率/mg/cm2平均值S11801801.6+0.1143.714743.65750.1910.194243.577943.51900.196S11651701.6+0.1341.380540.98491.3191.351442.284341.86941.383S10001701.6+0.1544.849744.80740.1410.138644.354044.31360.135S1000-21501.2+0.1732.499632.43890.2020.199832.158532.09980.196垂直沉銅線除膠流程（1）.4#程序（23#溶脹7分鐘）

①.藥水狀態(tài)及處理時(shí)間缸位藥水濃度溫度/°c處理時(shí)間/sec溶脹(23#)SW-110：36.1%70390除膠Kmno:56g/l；4K2mno4:16g/l；NaOH:46.2g/l79780中和NU-121：2.08N40300②.除膠速率板材TG值/C板厚/mm測(cè)試片序號(hào)測(cè)前稱重/g測(cè)后稱重/g除膠速率/mg/cm2平均值S11701701.3+0.1133.293733.26020.1120.122233.653433.61410.131S11551501.3+0.1533.647233.56340.2790.283633.372933.28670.287S11411351.2+0.1729.815129.75310.2060.205829.663429.60230.204IT1401351.3+0.1934.598134.49720.3360.3361034.338334.23770.335（2）.5#程序（23#溶脹5分鐘+24#溶脹5.5分鐘）①.藥水狀態(tài)及處理時(shí)間缸位藥水濃度溫度/c處理時(shí)間/sec溶脹(23#)SW-110：36.1%70300溶脹（24#）SW-110：52.1%75330除膠Kmno:56g/l；4K2mno4:16g/l；NaOH:46.2g/l79780中和NU-121：2.08N40300②.除膠速率板材TG值/C板厚/mm測(cè)試片序號(hào)測(cè)前稱重/g測(cè)后稱重/g除膠速率/mg/cm2平均值S11801801.6+0.1142.792142.73050.2050.206242.750242.68830.206S11701701.3+0.1334.057733.97970.2600.256433.766133.69070.251S11651701.6+0.1541.296141.03250.8790.865

■642.035041.77940.852S11551501.1±0.1730.039429.96850.2360.240830.035829.96260.244S11411351.2±0.1933.074232.99060.2790.2771032.738732.65660.274S10001701.6±0.11144.421144.3650.1870.1851244.627444.57270.182S1000-21501.3±0.11331.489331.43180.1920.1901432.498132.44190.187IT1801801.4±0.11542.223542.16080.2090.2131642.321842.25700.216IT1581501.2±0.11732.671732.58950.2740.2641832.738632.66270.253IT1401351.2±0.11934.589834.48810.3390.3272034.743434.64890.315六、測(cè)試數(shù)據(jù)分析及結(jié)論1.水平沉銅線⑴.水平除膠一次，速度1.0m/min。，板材S1165IT140S1155S1141IT158S1170除膠速率/mg/cm20.5040.2580.1520.1140.0520.038⑵.水平除膠兩次，速度1.5m/min+1.0m/min。，板材S1165IT140S1155S1141S1000-2S1180S1170S1000IT180IT158除膠速率/mg/cm20.9410.4420.2370.1550.0950.090.0720.0690.550.064⑶.水平除膠兩次，速度1.0m/min+1.0m/min。，板材S1165IT140S1155S1141S1000-2S1180S1170S1000IT180IT158除膠速率/mg/cm21.1160.5330.2910.1640.1240.1120.0820.0920.0850.09⑷.垂直除膠+水平除膠，垂直除膠（溶脹8分鐘），水平除膠速度速度1.0m/min。板材S1165S1000-2S1180S1000IT180除膠速率/mg/cm21.3630.2180.1930.1610.175⑸.垂直除膠+水平除膠，垂直除膠（溶脹10分鐘?），水平除膠速度速度1.0m/min。板材S1165S1000-2S1180S1000除膠速率/mg/cm21.3510.1990.1940.138羅門哈司藥水商對(duì)水平沉銅線除膠速率控制的建議，普通TG板材的除膠速率控制在0.1一0.3mg/cm2之間，高TG板材的除膠速率控制在0.05—0.15mg/cm2之間。根據(jù)該建議及數(shù)據(jù)分析，第⑴種除膠流程適合生產(chǎn)IT140板材的板；第⑵種除膠流程適合生產(chǎn)S1141、S1000-2板材的板；第⑶、⑷、⑸除膠流程適合生產(chǎn)