基于分子識(shí)別的農(nóng)產(chǎn)品中有機(jī)磷農(nóng)藥新型檢測技術(shù)研究與應(yīng)用

1、序號(hào)知識(shí)產(chǎn)權(quán)名稱知識(shí)產(chǎn)權(quán)類別發(fā)明人知識(shí)產(chǎn)權(quán)人知識(shí)產(chǎn)權(quán)號(hào)取得日期國（區(qū)）別發(fā)明專利有效狀態(tài)證明材料1一種同時(shí)檢測九種有機(jī)磷農(nóng)藥的方法發(fā)明專利權(quán)徐志祥；王璽龍；趙濤山東農(nóng)業(yè)大學(xué)2014-8-6中國有效附件-12一種同時(shí)檢測敵百蟲和久效磷的方法發(fā)明專利權(quán)徐志祥；辛軍紅；喬旭光山東農(nóng)業(yè)大學(xué)2013-10-16中國有效附件-23一種酶標(biāo)記仿生免疫分析檢測敵百蟲和乙酰甲胺磷的方法發(fā)明專利權(quán)徐志祥；時(shí)辰；高繪菊山東農(nóng)業(yè)大學(xué)2016-9-21中國有效附件-34敵百蟲仿生酶聯(lián)免疫吸附檢測方法發(fā)明專利權(quán)徐志祥；孟玲；喬旭光山東農(nóng)業(yè)大學(xué)2013-7-31中國有效附件-4序號(hào)論文專著名稱發(fā)表刊物（出版社）發(fā)表（出版）

2、時(shí)間作者（按刊物發(fā)表順序）證明材料1Study of an online molecularly imprinted solid phase extraction coupled to chemiluminescence sensor for the determination of trichlorfon in vegetablesJournal of Agricultural and Food Chemistry2011-12Ling Meng; Xuguang Qiao; Jiaming Song; Zhixiang Xu*; Junhong Xin; Yue Zhang附件-52Sim

3、ultaneous determination of nine trace organophosphorous pesticide residues in fruit samples using molecularly imprinted matrix solid-phase dispersion followed by gas chromatographyJournal of Agricultural and Food Chemistry2013-4Xilong Wang; Xuguang Qiao; Yue Ma; Tao Zhao; Zhixiang Xu*附件-63Simultaneo

4、us separation and determination of 8 organophosphorous pesticide residues in vegetables through molecularly imprinted solid-phase extraction coupled to gas chromatographyJournal of Separation Science2012-12Junhong Xin; Xuguang Qiao; Yue Ma; Zhixiang Xu*附件-74Molecularly imprinted polymer as sorbent f

5、or solid-phase extraction coupling to gas chromatography for the simultaneous determination of trichlorfon and monocrotophos residues in vegetablesFood Analytical Methods2013-1Junhong Xin; Xuguang Qiao; Zhixiang Xu*; Jie Zhou附件-85Simultaneous determination of three trace organophosphorus pesticide r

6、esidues in vegetables using molecularly imprinted solid-phase extraction coupled with high performance liquid chromatographyFood Analytical Methods2016-1Qingqing Wang; Xin Zhang#; Zhixiang Xu; Huiju Gao*附件-96Molecularly imprinted solid-phase extraction coupled with high-performance liquid chromatogr

7、aphy for the determination of trace trichlorfon and monocrotophos residues in fruitsFood Analytical Methods2017-4Deqing Li; Xin Zhang#; Feifan Kong; Xuguang Qiao*; Zhixiang Xu*附件-107Development of a direct competitive biomimetic enzyme-linked immunosorbent assay based on a hydrophilic molecularly im

8、printed membrane for the determination of trichlorfon residues in vegetablesFood Analytical Methods2012-9Ling Meng; Xuguang Qiao; Zhixiang Xu*; Junhong Xin; Lei Wang附件-118A study on biomimetic immunoassay-capillary electrophoresis method based on molecularly imprinted polymer for determination of tr

9、ace trichlorfon residue in vegetablesFood Chemistry2016-12Jie Li; Juxiu Lu#; Xuguang Qiao*; Zhixiang Xu*附件-129The biomimetic immunoassay based on molecularly imprinted polymer: A comprehensive review of recent progress and future prospectsJournal of Food Science2011-3Zhixiang Xu; Huiju Gao; Limin Zh

10、ang; Xueqing Chen; Xuguang Qiao*附件-1310Development of molecularly imprinted electrochemical sensors based on Fe3O4MWNTs-COOH/CS nanocomposite layers for detecting traces of acephate and trichlorfonAnalyst2014-11Qinghua Tang; Xiujuan Shi#; Xiaolin Hou; Jie Zhou; Zhixiang Xu*附件-14姓名排序職稱工作單位對(duì)成果創(chuàng)造性貢獻(xiàn)曾獲省

11、級(jí)以上科技獎(jiǎng)勵(lì)情況徐志祥1/6教授山東農(nóng)業(yè)大學(xué)主持人，負(fù)責(zé)項(xiàng)目整體設(shè)計(jì)實(shí)施、協(xié)調(diào)，對(duì)創(chuàng)新點(diǎn)一、二、三、四做出了創(chuàng)造性貢獻(xiàn)。制備了高選擇性的分子印跡吸附功能材料和識(shí)別元件，并對(duì)吸附性能進(jìn)行表征；優(yōu)化了與色譜、化學(xué)發(fā)光體系、毛細(xì)管電泳、電化學(xué)傳感器的匹配性，解決了化學(xué)反應(yīng)與生化反應(yīng)的協(xié)同性，建立了農(nóng)產(chǎn)品等復(fù)雜基質(zhì)中有機(jī)磷農(nóng)藥殘留高精準(zhǔn)檢測新方法；研發(fā)了MI-SPE有機(jī)磷農(nóng)藥專用固相萃取柱產(chǎn)品。無喬旭光2/6教授山東農(nóng)業(yè)大學(xué)本項(xiàng)目主要成員，負(fù)責(zé)項(xiàng)目的技術(shù)指導(dǎo)和實(shí)施，對(duì)創(chuàng)新點(diǎn)一、二、三有創(chuàng)造性貢獻(xiàn)。具體參與高選擇性的分子印跡吸附功能材料的表征；有機(jī)磷農(nóng)藥痕量殘留分子印跡吸附檢測方法的建立及其在農(nóng)產(chǎn)品等

12、復(fù)雜基質(zhì)有機(jī)磷農(nóng)藥殘留檢測中的應(yīng)用。無高繪菊3/6副教授山東農(nóng)業(yè)大學(xué)本項(xiàng)目主要成員，負(fù)責(zé)項(xiàng)目的實(shí)施，對(duì)創(chuàng)新點(diǎn)二、三有創(chuàng)造性貢獻(xiàn)。具體負(fù)責(zé)仿生抗體的制備及性能表征；仿生免疫分析以及仿生電化學(xué)傳感器檢測方法的建立及其在實(shí)際樣品檢測中的應(yīng)用與方法評(píng)價(jià)。無張麗敏4/6講師山東農(nóng)業(yè)大學(xué)本項(xiàng)目技術(shù)骨干，負(fù)責(zé)項(xiàng)目的實(shí)施，對(duì)創(chuàng)新點(diǎn)一有創(chuàng)造性貢獻(xiàn)，創(chuàng)新點(diǎn)二做出了重要貢獻(xiàn)。具體負(fù)責(zé)對(duì)敵百蟲等具有高選擇識(shí)別能力的分子印跡毛細(xì)管整體柱的制備；分子印跡固相萃取與毛細(xì)管電泳聯(lián)用檢測葡萄酒中有機(jī)磷農(nóng)藥新方法的建立及應(yīng)用。無孔非凡5/6高級(jí)工程師山東五洲檢測 本項(xiàng)目技術(shù)骨干，負(fù)責(zé)項(xiàng)目的實(shí)施，對(duì)創(chuàng)新點(diǎn)四做出了重要貢獻(xiàn)。參與MI-SPE有機(jī)磷專用固相萃取柱性能改善與產(chǎn)品研發(fā)，有機(jī)磷農(nóng)藥多殘留仿生檢測技術(shù)集成；負(fù)責(zé)有機(jī)磷農(nóng)藥殘留高