DB43-T 2296-2022地理標(biāo)志產(chǎn)品 德山大曲

ICS67.160.10

CCSX62

43

湖南省地方標(biāo)準(zhǔn)

DB43/T2296—2022

地理標(biāo)志產(chǎn)品德山大曲

ProductofgeographicalindicationDeshanDaqu

2022-03-02發(fā)布2022-05-02實(shí)施

湖南省市場(chǎng)監(jiān)督管理局發(fā)布

DB43/T2296—2022

目次

前言························································································································Ⅲ

引言························································································································Ⅴ

1范圍·····················································································································1

2規(guī)范性引用文件······································································································1

3術(shù)語和定義············································································································1

4保護(hù)范圍···············································································································2

5原輔料要求············································································································2

6加工要求···············································································································2

7質(zhì)量要求···············································································································3

8檢驗(yàn)方法···············································································································4

9檢驗(yàn)規(guī)則···············································································································5

10標(biāo)志、標(biāo)簽、包裝、運(yùn)輸和貯存···············································································6

附錄A（規(guī)范性）德山大曲地理標(biāo)志產(chǎn)品保護(hù)范圍區(qū)域圖··················································7

參考文獻(xiàn)····················································································································8

I

DB43/T2296—2022

前言

本文件按照GB/T1.1—2020《標(biāo)準(zhǔn)化工作導(dǎo)則第1部分：標(biāo)準(zhǔn)化文件的結(jié)構(gòu)和起草規(guī)則》的規(guī)

定起草。

請(qǐng)注意本文件的某些內(nèi)容可能涉及專利，本文件的發(fā)布機(jī)構(gòu)不承擔(dān)識(shí)別這些專利的責(zé)任。

本文件由湖南省知識(shí)產(chǎn)權(quán)局提出。

本文件由湖南省地理標(biāo)志產(chǎn)品標(biāo)準(zhǔn)化技術(shù)委員會(huì)歸口。

本文件起草單位：常德經(jīng)濟(jì)技術(shù)開發(fā)區(qū)德山大曲地理標(biāo)志產(chǎn)品保護(hù)管理辦公室、常德經(jīng)濟(jì)技術(shù)開發(fā)

區(qū)市場(chǎng)監(jiān)督管理局、湖南德山酒業(yè)有限公司、湖南天擇質(zhì)量技術(shù)服務(wù)有限公司。

本文件主要起草人：郭志強(qiáng)、曾鐵軍、高翔、鄭慧平、許向陽、萬濤、向陽、左中文、楊軍、張建

平、王宏兵、劉衛(wèi)東。

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DB43/T2296—2022

引言

“德山大曲釀造技藝”起源于距今7000—9000年的澧縣城頭山。城頭山人所創(chuàng)造的釀酒技藝從富

饒的澧水流域經(jīng)浩瀚的洞庭湖輾轉(zhuǎn)流傳到沅水流域，并在桃源縣落地生根，發(fā)揚(yáng)光大，形成為自北魏至

宋代史不絕書的武陵桃源酒法。唐代，沅水流域的漢壽毛家灘李氏釀酒作坊采用“古法釀造、量質(zhì)接酒、

分級(jí)裝壇、多年貯存”的方式釀酒，所產(chǎn)“鏡面酒”、“堆花酒”在宋代曾被欽定為貢酒。后來李氏釀酒

技藝流傳到位于常德城東門外水府廟的馬萬隆糟坊，從清朝到民國(guó)，經(jīng)過五代相傳與發(fā)展，成為常德正

宗古法釀酒技藝之集大成者。

1952年以馬萬隆糟坊為基礎(chǔ)成立的德山酒廠采用該項(xiàng)技藝釀造出窖香突出、爽凈柔順的濃香型白

酒“德山大曲”獲得成功，并在1963年、1984年、1988年三次全國(guó)評(píng)酒會(huì)上獲得銀質(zhì)獎(jiǎng)。至此，“德

山大曲”聲譽(yù)日隆，被譽(yù)為“瀟湘第一濃香酒”，也是常德地區(qū)最富特色的白酒產(chǎn)品之一。

V

DB43/T2296—2022

地理標(biāo)志產(chǎn)品德山大曲

1范圍

本文件規(guī)定了德山大曲的保護(hù)范圍、原輔料要求、加工要求、質(zhì)量要求、檢驗(yàn)方法、檢驗(yàn)規(guī)則、標(biāo)

志、標(biāo)簽、包裝、運(yùn)輸和貯存的要求。

本文件適用于地理標(biāo)志產(chǎn)品德山大曲白酒的生產(chǎn)和銷售。

2規(guī)范性引用文件

下列文件中的內(nèi)容通過文中的規(guī)范性引用而構(gòu)成本文件必不可少的條款。其中，注日期的引用文件，

僅該日期對(duì)應(yīng)的版本適用于本文件；不注日期的引用文件，其最新版本（包括所有的修改單）適用于本

文件。

GB1351小麥

GB1353玉米

GB/T1354大米

GB2757食品安全國(guó)家標(biāo)準(zhǔn)蒸餾酒及其配制酒

GB5009.225食品安全國(guó)家標(biāo)準(zhǔn)酒中乙醇濃度的測(cè)定

GB5749生活飲用水衛(wèi)生標(biāo)準(zhǔn)

GB7718食品安全國(guó)家標(biāo)準(zhǔn)預(yù)包裝食品標(biāo)簽通則

GB/T8231高粱

GB8951食品安全國(guó)家標(biāo)準(zhǔn)蒸餾酒及其配制酒生產(chǎn)衛(wèi)生規(guī)范

GB/T10345—2007白酒分析方法

GB/T10346白酒檢驗(yàn)規(guī)則和標(biāo)志、包裝、運(yùn)輸、貯存

GB12456食品安全國(guó)家標(biāo)準(zhǔn)食品中總酸的測(cè)定

GB/T15109白酒工業(yè)術(shù)語

GB/T17924地理標(biāo)志產(chǎn)品標(biāo)準(zhǔn)通用要求

GB31621食品安全國(guó)家標(biāo)準(zhǔn)食品經(jīng)營(yíng)過程衛(wèi)生規(guī)范

JJF1070定量包裝商品凈含量計(jì)量檢驗(yàn)規(guī)則

QB/T4259濃香大曲

3術(shù)語和定義

GB/T15109界定的以及下列術(shù)語和定義適用于本文件。

3.1

德山大曲DeshanDaqu

在規(guī)定的保護(hù)范圍內(nèi)，以當(dāng)年出產(chǎn)高粱、小麥、糯米、大米、玉米為原料，經(jīng)粉碎、潤(rùn)料、混蒸

混燒、攤涼下曲、入池發(fā)酵、再混蒸混燒、分級(jí)裝壇、貯存勾兌而成的具有窖香突出、爽凈柔順的濃香

型白酒。

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4保護(hù)范圍

湖南省常德經(jīng)濟(jì)技術(shù)開發(fā)區(qū)德山街道辦事處、樟木橋街道辦事處和石門橋鎮(zhèn)現(xiàn)轄行政區(qū)域。（詳見

附錄A）

5原輔料要求

5.1高粱

當(dāng)年出產(chǎn)，符合GB/T8231規(guī)定的優(yōu)質(zhì)紅高粱。

5.2小麥

當(dāng)年出產(chǎn)，符合GB1351規(guī)定的軟質(zhì)小麥。

5.3大米、糯米

當(dāng)年出產(chǎn)，符合GB/T1354規(guī)定的優(yōu)質(zhì)大米、糯米。

5.4玉米

當(dāng)年出產(chǎn)，符合GB1353規(guī)定的優(yōu)質(zhì)玉米

5.5曲塊

當(dāng)年出產(chǎn)，符合QB/T4259規(guī)定。

5.6釀造用水

取自保護(hù)區(qū)域內(nèi)的地下水、山泉水和江河飲用水等天然優(yōu)質(zhì)水，水質(zhì)應(yīng)符合GB5749的規(guī)定。

5.7加漿用水

取自保護(hù)區(qū)域內(nèi)的地下水、山泉水和江河飲用水等天然優(yōu)質(zhì)水，pH6.5～7.0，總硬度70ppm～

90ppm，水質(zhì)應(yīng)符合GB5749的規(guī)定。

5.8粗殼

當(dāng)年生產(chǎn)，谷黃色，無霉變、異味，水分≤14%。

6加工要求

6.1工藝流程

原料→粉碎→潤(rùn)料→混料蒸酒→攤涼→下曲發(fā)酵→貯存→勾兌（勾調(diào)）→灌裝→產(chǎn)品。

6.2關(guān)鍵工藝要求

6.2.1原料

原料粉碎不宜太細(xì)，通過0.85mm（過濾篩）的量≥85%；粗殼預(yù)蒸最少保持30min，蒸透，無雜味。

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6.2.2混料蒸酒

酒糟和原料進(jìn)行拌和，要求拌散、和勻、無疙瘩、無灰包，拌好堆置30min后開始上甑蒸酒，接

酒時(shí)，酒精度控制在60％vol以上，流酒溫度控制在30℃以下，流速為2kg/min～3kg/min。

6.2.3攤涼

將蒸好的糧糟置于晾糟床上，翻動(dòng)2次～3次，并用鼓風(fēng)機(jī)將糧糟溫度吹冷至21℃～25℃。

6.2.4下曲發(fā)酵

采用固態(tài)發(fā)酵法，下曲溫度控制在21℃～25℃，入池溫度控制在16℃～21℃，發(fā)酵周期為45

天～90天。再進(jìn)行混料蒸酒。

6.2.5貯存

將蒸出來的酒貯存于地下酒窖的陶壇中，地下酒窖溫度控制在30℃以下，相對(duì)濕度控制在75%左

右，貯存時(shí)間≥3年。將此酒作為勾兌用的基酒。

6.2.6勾兌（勾調(diào)）

貯存時(shí)間≥3年以上，各種等級(jí)和口感風(fēng)格的基酒，先進(jìn)行小樣勾兌（勾調(diào)），小樣口感、理化指

標(biāo)符合要求后按小樣比列勾兌（勾調(diào)）大樣。大樣理化指標(biāo)檢驗(yàn)合格后，封存罐儲(chǔ)1個(gè)月。

6.2.7灌裝

將罐儲(chǔ)1個(gè)月的酒體送檢，檢驗(yàn)合格后方能灌裝出廠。

6.3生產(chǎn)加工的衛(wèi)生要求

生產(chǎn)過程衛(wèi)生應(yīng)符合GB8951規(guī)定。

7質(zhì)量要求

7.1感官要求

感官要求應(yīng)符合表1的規(guī)定。

表1感官要求

項(xiàng)目要求

色澤和外觀無色或微黃，清亮透明，無懸浮物，無沉淀

香氣窖香突出、輔以幽雅陳香、形成豐滿的復(fù)合香味，無異味

口味酒體醇和協(xié)調(diào)、細(xì)膩、后味柔順

風(fēng)格具有本品典型的風(fēng)格

雜質(zhì)無正常視力可見外來雜質(zhì)

注：當(dāng)酒的溫度低于10℃時(shí)，允許出現(xiàn)白色絮狀沉淀物質(zhì)或失光。10℃以上時(shí)應(yīng)逐漸恢復(fù)正常。

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7.2理化指標(biāo)

理化指標(biāo)應(yīng)符合表2的規(guī)定。

表2理化指標(biāo)

項(xiàng)目指標(biāo)

酒精度（20℃）/（%vol)52±1

總酸（以乙酸計(jì)）/（g/L)≥0.4

總酯（以乙酸乙酯計(jì)）/（g/L）≥2.0

己酸乙酯/（g/L）1.2～2.2

固形物/（g/L）≤0.4

7.3安全要求

應(yīng)符合GB2757的規(guī)定。

7.4凈含量

應(yīng)符合國(guó)家質(zhì)量監(jiān)督檢驗(yàn)檢疫總局令【2005】第75號(hào)《定量包裝商品計(jì)量監(jiān)督管理辦法》的規(guī)定。

8檢驗(yàn)方法

8.1感官要求

按GB/T10345—2007第5章的規(guī)定執(zhí)行。

8.2酒精度

按GB5009.225的規(guī)定執(zhí)行。

8.3總酸

按GB12456的規(guī)定執(zhí)行。

8.4總酯

按GB/T10345—2007第8章的規(guī)定執(zhí)行。

8.5己酸乙酯

按GB/T10345—2007的第11章規(guī)定執(zhí)行

8.6固形物

按GB/T10345—2007第9章的規(guī)定執(zhí)行。

8.7安全要求

按GB2757的規(guī)定的檢驗(yàn)方法執(zhí)行。

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8.8凈含量

按JJF1070的規(guī)定執(zhí)行。

9檢驗(yàn)規(guī)則

9.1組批

同一原料、同一生產(chǎn)線、同一品種、同一生產(chǎn)日期為一個(gè)檢驗(yàn)批次。

9.2抽樣方法

9.2.1按表3抽取樣本，從每箱中任取一瓶，單瓶包裝凈含量＜500ml，總?cè)恿浚?500ml時(shí)，可

按比例增加抽樣量。

表3抽樣表

批量范圍/箱樣本數(shù)/箱單位樣本數(shù)/瓶

＜5033

50～120052

1201～3500081

＞35000131

9.2.2采樣后應(yīng)立即貼上標(biāo)簽，注明：樣品名稱、品種規(guī)格、數(shù)量、制造者名稱、采樣時(shí)間與地點(diǎn)、

采樣人。將樣品分為兩份，一份樣品封存，保留（2年）備查。另一份樣品立即送化驗(yàn)室進(jìn)行感官、

理化檢驗(yàn)。

9.3出廠檢驗(yàn)

9.3.1每批產(chǎn)品應(yīng)經(jīng)生產(chǎn)企業(yè)質(zhì)量部門檢驗(yàn)，檢驗(yàn)合格后方能出廠。

9.3.2出廠檢驗(yàn)項(xiàng)目為：感官、酒精度、總酸、總酯、己酸乙酯、固形物、凈含量。

9.4型式檢驗(yàn)

型式檢驗(yàn)內(nèi)容包含本文件規(guī)定的全部?jī)?nèi)容，每年應(yīng)進(jìn)行一次，有下列情形之一者應(yīng)進(jìn)行型式檢驗(yàn)：

a）申請(qǐng)使用地理標(biāo)志產(chǎn)品保護(hù)專用標(biāo)志時(shí)；

b）更換關(guān)鍵生產(chǎn)設(shè)備時(shí)；

c）停產(chǎn)3個(gè)月后，重新恢復(fù)生產(chǎn)時(shí)；

d）出廠檢驗(yàn)與上次型式檢驗(yàn)結(jié)果有較大差異時(shí)；

e）產(chǎn)品監(jiān)督管理機(jī)構(gòu)提出要求時(shí)。

9.5判定規(guī)則

9.5.1產(chǎn)品檢驗(yàn)項(xiàng)目全部符合本文件要求時(shí)，判定為合格品。

9.5.2產(chǎn)品檢驗(yàn)項(xiàng)目中如有一項(xiàng)或一項(xiàng)以上不符合本文件要求時(shí)，應(yīng)在該批次產(chǎn)品留樣中取樣復(fù)檢。

復(fù)檢結(jié)果符合本文件要求，判定為合格品，復(fù)檢結(jié)果仍不符合文件要求，判定為不合格品。

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10標(biāo)志、標(biāo)簽、包裝、運(yùn)輸和貯存

10.1標(biāo)志、標(biāo)簽

應(yīng)符合GB2757、GB7718和GB/T17924的有關(guān)規(guī)定。地理標(biāo)志專用標(biāo)志應(yīng)符合地理標(biāo)志專用標(biāo)志

使用管理相關(guān)規(guī)定。

10.2包裝

應(yīng)符合GB31621、GB/T10346的規(guī)定。

10.3運(yùn)輸

應(yīng)符合GB31621、GB/T10346的規(guī)定。

10.4貯存

應(yīng)符合GB31621、GB/T10346的規(guī)定。

6

DB43/T2296—2022

附錄A

（規(guī)范性）

德山大曲地理標(biāo)志產(chǎn)品保護(hù)范圍區(qū)域圖

德山大曲地理標(biāo)志產(chǎn)品保護(hù)范圍區(qū)域圖如圖A.1所示。

圖A.1德山大曲地理標(biāo)志產(chǎn)品保護(hù)范圍區(qū)域圖

7

DB43/T2296—2022

參考文獻(xiàn)

[1]國(guó)家質(zhì)量監(jiān)督檢驗(yàn)檢疫總局令〔2005〕第75號(hào)《定量包裝商品計(jì)量監(jiān)督管理辦法》

[2]國(guó)家質(zhì)量監(jiān)督檢驗(yàn)檢疫總局公告〔2005〕第151號(hào)《地理標(biāo)志產(chǎn)品保護(hù)專用標(biāo)志》

8

DB43/T2296—2022

目次

前言························································································································Ⅲ

引言························································································································Ⅴ

1范圍·····················································································································1

2規(guī)范性引用文件······································································································1

3術(shù)語和定義············································································································1

4保護(hù)范圍···············································································································2

5原輔料要求············································································································2

6加工要求···············································································································2

7質(zhì)量要求···············································································································3

8檢驗(yàn)方法···············································································································4

9檢驗(yàn)規(guī)則···············································································································5

10標(biāo)志、標(biāo)簽、包裝、運(yùn)輸和貯存···············································································6

附錄A（規(guī)范性）德山大曲地理標(biāo)志產(chǎn)品保護(hù)范圍區(qū)域圖··················································7

參考文獻(xiàn)··································································