南京土壤檢測(cè)中心-CNAS

1、ISO/IEC 17025 認(rèn)可證書(shū) CNAS-PD20/09-B/1中國(guó)合格評(píng)定國(guó)家認(rèn)可委員會(huì)認(rèn) 可 證 書(shū) 附 件（注冊(cè)號(hào)：CNAS L2464）名稱: 中國(guó)科學(xué)院南京土壤研究所土壤與環(huán)境分析測(cè)試中心 地址：江蘇省南京市北京東路71號(hào)簽發(fā)日期：2010年12月10日 有效期至：2013年12月09日更新日期：2012年04月09日附件1 認(rèn)可的授權(quán)簽字人及領(lǐng)域序號(hào)姓 名授權(quán)簽字領(lǐng)域備 注1章鋼婭土壤、空氣、植物與食品、水、肥料的檢測(cè)項(xiàng)目2曹亞澄土壤、空氣、植物與食品、水、肥料的檢測(cè)項(xiàng)目CHINA NATIONAL ACCREDITATION SERVICE FOR CONFORMITY A

2、SSESSMENTAPPENDIX OF ACCREDITATION CERTIFICATE(Registration No. CNAS L2464) NAME:Soil and Environment Analysis Center of Nanjing Institute of Soil Science, Chinese Academy of Sciences ADDRESS:No.71, Beijing East Road, Nanjing, Jiangsu, ChinaDate of Issue:2010-12-10 Date of Expiry:2013-12-09 Date of

3、Update：2012-04-09APPENDIX 1 ACCREDITED SIGNATORIES AND SCOPEName Authorized Scope of SignatureNote1Zhang GangyaAll approved projects2Cao YachengAll approved projects 中國(guó)合格評(píng)定國(guó)家認(rèn)可委員會(huì)認(rèn) 可 證 書(shū) 附 件（注冊(cè)號(hào)：CNAS L2464）名稱: 中國(guó)科學(xué)院南京土壤研究所土壤與環(huán)境分析測(cè)試中心 地址：江蘇省南京市北京東路71號(hào)認(rèn)可依據(jù)：ISO/IEC 17025:2005以及CNAS特定認(rèn)可要求簽發(fā)日期：2010年12月10

4、日 有效期至：2013年12月09日更新日期：2012年04月09日附件2 認(rèn)可的檢測(cè)能力范圍序號(hào)檢測(cè)對(duì)象項(xiàng)目/參數(shù)領(lǐng)域代碼檢測(cè)標(biāo)準(zhǔn)（方法）名稱及編號(hào)（含年號(hào)）限制范圍說(shuō)明序號(hào)名稱1土壤1pH0238LY/T 1239-1999 森林土壤pH值的測(cè)定2有機(jī)質(zhì)0238LY/T 1237-1999 森林土壤有機(jī)質(zhì)的測(cè)定及碳氮比的計(jì)算3水分0238LY/T1213-1999森林土壤含水量的測(cè)定4全氮0238NY/T 53-1987土壤全氮測(cè)定法(半微量凱氏法)1土壤5全磷0238LY/T 1232-1999森林土壤全磷的測(cè)定6有效磷0238LY/T 1233-1999森林土壤有效磷的測(cè)定7全鉀023

5、8LY/T 1234-1999森林土壤全鉀的測(cè)定8速效鉀0238LY/T 1236-1999森林土壤速效鉀的測(cè)定9水溶性 鹽分0238LY/T 1251-1999森林土壤水溶性鹽分分析10有效銅0238LY/T 1260-1999森林土壤有效銅的測(cè)定11有效鋅0238LY/T 1261-1999森林土壤有效鋅的測(cè)定12有效鐵0238LY/T 1262-1999森林土壤有效鐵的測(cè)定13六六六、 滴滴涕0238GB/T 14550-2003土壤中六六六和滴滴涕測(cè)定的氣相色譜法14碳穩(wěn)定性同位素比值0238有機(jī)化合物的碳同位素質(zhì)譜分析土壤農(nóng)業(yè)化學(xué)分析方法中國(guó)農(nóng)業(yè)科技出版社，1999年，564-570

6、頁(yè)15氮穩(wěn)定性同位素比值0238氮同位素質(zhì)譜分析土壤農(nóng)業(yè)化學(xué)分析方法中國(guó)農(nóng)業(yè)科技出版社，1999年，558-564頁(yè)。16總鉻0238HJ 4912009土壤 總鉻的測(cè)定 火焰原子吸收分光光度法不用6.2.21土壤17鉛, 鎘0238GB/T 171411997土壤質(zhì)量 鉛、鎘的測(cè)定 石墨爐原子吸收分光光度法18銅, 鋅0238GB/T 171381997土壤質(zhì)量 銅、鋅的測(cè)定 火焰原子吸收分光光度法19總汞0238GB/T 22105.1-2008土壤質(zhì)量 總汞、總砷、總鉛的測(cè)定 原子熒光法 第1部分：土壤中總汞的測(cè)定20總砷0238GB/T 22105.2-2008土壤質(zhì)量 總汞、總砷、總

7、鉛的測(cè)定 原子熒光法 第2部分：土壤中總砷的測(cè)定21電導(dǎo)率0238DIN ISO 11265-1997 土壤質(zhì)量.特定電導(dǎo)率的測(cè)定22水解性氮0238LY/T 1229-1999 森林土壤水解性氮的測(cè)定23銨態(tài)氮、硝態(tài)氮、亞硝態(tài)氮0238ISO 14256-2-2005土壤質(zhì)量-氯化鉀萃取法測(cè)定潮濕土壤中的硝酸鹽、亞硝酸鹽和氨鹽基的含量-第2部分: 以分段流程分析進(jìn)行的自動(dòng)測(cè)定方法24氯離子0238NY/T 1121.17-2006 土壤檢測(cè) 第17部分：土壤氯離子含量的測(cè)定 僅用前處理方法24氯離子0238HJ/T 84-2001 水質(zhì) 無(wú)機(jī)陰離子的測(cè)定 離子色譜法僅用測(cè)定方法1土壤25硫酸

8、根離子0238NY/T 1121.18-2006 土壤檢測(cè) 第18部分:土壤硫酸根離子含量的測(cè)定HJ/T84-2001 水質(zhì) 無(wú)機(jī)陰離子的測(cè)定 離子色譜法26礦質(zhì)全量0238偏硼酸鋰熔融-ICP-AES法 土壤農(nóng)業(yè)化學(xué)分析方法中國(guó)農(nóng)業(yè)科技出版社，1999年，45-47頁(yè)。27全鈣、鎂、鈉0238NY/T 296-1995土壤全鈣、鎂、鈉的測(cè)定28鎳0238GB/T 17139-1997土壤質(zhì)量 鎳的測(cè)定 火焰原子吸收分光光度法29全硒0238NY/T 1104-2006 土壤中全硒的測(cè)定 原子熒光光度法30有機(jī)磷農(nóng)藥0238GB/T 14552-2003水和土壤質(zhì)量 有機(jī)磷農(nóng)藥的測(cè)定 氣相色譜

9、法31石油烴0238GB/T 17378.5-2007 海洋監(jiān)測(cè)規(guī)范 第5部分:沉積物分析2空氣32空氣中N2O氮、氧同位素比值0238GB/T 6041-2002質(zhì)譜分析方法通則； 大氣濃度下N2O、CH4和CO2中氮、碳和氧穩(wěn)定同位素比值的質(zhì)譜測(cè)定，土壤學(xué)報(bào)，2008,第45卷，第2期，249-258頁(yè)。2空氣33空氣中CH4碳同位素比值0238GB/T 6041-2002質(zhì)譜分析方法通則； 大氣濃度下N2O、CH4和CO2中氮、碳和氧穩(wěn)定同位素比值的質(zhì)譜測(cè)定，土壤學(xué)報(bào)，2008,第45卷，第2期，249-258頁(yè)。34氣體中N2氮同位素比值023835空氣中CO2碳、氧同位素比值0238

10、36氣體中CH4含量0238GB/T 8984-2008氣體中一氧化碳、二氧化碳和碳?xì)浠衔锏臏y(cè)定第1部分：氣體中一氧化碳、二氧化碳和甲烷的測(cè)定氣相色譜法37氣體中CO2含量0238GB/T 18204.24-2000 氣體中一氧化碳、二氧化碳和碳?xì)浠衔锏臏y(cè)定3植物與食品38六六六、 滴滴涕0227GB/T5009.19-2008食品中有機(jī)氯農(nóng)藥多組分殘留量的測(cè)定39植物粗灰分的測(cè)定0244GB/T5009.4-2010食品中灰分的測(cè)定40全氮0227LY/T 1269-1999森林植物與森林枯枝落葉層全氮的測(cè)定3植物與食品41全磷0227LY/T 1271-1999 森林植物與森林枯枝落葉

11、層全氮、磷、鉀、鈉、鈣、鎂的測(cè)定42全鉀0227LY/T 1271-1999 森林植物與森林枯枝落葉層全氮、磷、鉀、鈉、鈣、鎂的測(cè)定43鎘0227GB/T 5009.15-2003食品中鎘的測(cè)定只做第一法44總汞0227GB/T 5009.17-2003食品中總汞及有機(jī)汞的測(cè)定只做第一法45鉛0227GB/T5009.12-2010食品中鉛的測(cè)定只做第一法46硒0227GB 5009.932010 食品安全國(guó)家標(biāo)準(zhǔn)食品中硒的測(cè)定只做第一法47碳穩(wěn)定性同位素比值0244有機(jī)化合物的碳同位素質(zhì)譜分析土壤農(nóng)業(yè)化學(xué)分析方法中國(guó)農(nóng)業(yè)科技出版社，1999年，564-570頁(yè)48氮穩(wěn)定性同位素比值0244氮

12、同位素質(zhì)譜分析土壤農(nóng)業(yè)化學(xué)分析方法中國(guó)農(nóng)業(yè)科技出版社，1999年，558-564頁(yè)。4水49pH0238GB/T 6920-1986水質(zhì) pH值的測(cè)定 玻璃電極法50銅，鋅， 鉛，鎘0238GB/T 7475-1987水質(zhì) 銅，鋅，鉛，鎘的測(cè)定 原子吸收分光光度法4水51銨0238ISO 11732-2005 水質(zhì) 氨氮的測(cè)定.流動(dòng)分析(CFA和FIA)和光譜測(cè)定法52硝酸鹽氮0238ISO 13395-1996 水質(zhì)用流動(dòng)分析(CFA 和FIA)和光譜檢測(cè)法測(cè)定水中亞硝酸鹽氮和硝酸鹽氮及二者的總量53電導(dǎo)率0238DZ/T0064.6-1993地下水質(zhì)檢測(cè)方法電導(dǎo)率的測(cè)定54全鹽量0238H

13、J/T 51-1999水質(zhì) 全鹽量的測(cè)定 重量法55全鉀0238EPA 200.7 水、固體、生物固體 痕量元素的測(cè)定 電感耦合等離子體原子發(fā)射光譜法56碳酸根、重碳酸根0238DZ/T0064.49-1993地下水質(zhì)檢測(cè)方法 滴定法測(cè)定碳酸根、重碳酸根和氫氧根57氯離子和 硫酸根0238HJ/T84-2001 水質(zhì) 無(wú)機(jī)陰離子的測(cè)定 離子色譜法58磷酸鹽0238ISO 10304-1-2007 水質(zhì)-用離子色譜法測(cè)定溶解的陰離子-第1部分：溴化物、氯化物、氟化物、硝酸鹽、亞硝酸鹽、磷酸鹽和硫酸鹽的測(cè)定4水59鋁0238EPA 200.7 水、固體、生物固體 痕量元素的測(cè)定 電感耦合等離子體原

14、子發(fā)射光譜法60鈣、鎂0238EPA 200.7 水、固體、生物固體 痕量元素的測(cè)定 電感耦合等離子體原子發(fā)射光譜法61鐵、錳0238EPA 200.7 水、固體、生物固體 痕量元素的測(cè)定 電感耦合等離子體原子發(fā)射光譜法62汞0238SL 327.2-2005 水質(zhì) 汞的測(cè)定 原子熒光光度法63鈉0238EPA 200.7 水、固體、生物固體 痕量元素的測(cè)定 電感耦合等離子體原子發(fā)射光譜法64鎳0238EPA 200.7 水、固體、生物固體 痕量元素的測(cè)定 電感耦合等離子體原子發(fā)射光譜法65砷0238SL 327.1-2005 水質(zhì) 砷的測(cè)定 原子熒光光度法66硒0238SL 327.3-20

15、05 水質(zhì) 硒的測(cè)定 原子熒光光度法4水67六六六、 滴滴涕0238GB/T 7492-1987水質(zhì) 六六六、滴滴涕的測(cè)定 氣相色譜法68有機(jī)磷農(nóng)藥0238GB/T 14552-2003 水、土中有機(jī)磷農(nóng)藥測(cè)定的氣相色譜法69六價(jià)鉻0238GB/T 7467-1987水質(zhì) 六價(jià)鉻的測(cè)定 二苯碳酰二肼分光光度法5肥料70總氮0232GB/T 17767.1-2008有機(jī)-無(wú)機(jī)復(fù)混肥料的測(cè)定方法 第一部分:總氮含量71總磷0232GB/T 17767.2-2010有機(jī)無(wú)機(jī)復(fù)混肥料中總磷含量的測(cè)定72總鉀0232GB/T 17767.3-2010 有機(jī)-無(wú)機(jī)復(fù)混肥料中總鉀含量的測(cè)定73汞、砷、鎘、鉛

16、、鉻0232NY 1110-2006 水溶肥料汞、砷、鎘、鉛、鉻的限量及其含量測(cè)定No. CNAS L2464 第 28 頁(yè) 共 28 頁(yè) The scope of the accreditation in Chinese remains the definitive version. CHINA NATIONAL ACCREDITATION SERVICE FOR CONFORMITY ASSESSMENTAPPENDIX OF ACCREDITATION CERTIFICATE(Registration No. CNAS L2464) NAME:Soil and Environment A

17、nalysis Center of Nanjing Institute of Soil Science, Chinese Academy of Sciences ADDRESS:No.71, Beijing East Road, Nanjing, Jiangsu, ChinaAccreditation Criteria:ISO/IEC 17025:2005 and relevant requirements of CNASDate of Issue:2010-12-10 Date of Expiry:2013-12-09 Date of Update：2012-04-09APPENDIX 2

18、ACCREDITED TESTINGTest ObjectItem/ParameterCode of Field Title, Code of Standard or Method Limitation NoteItem/ Parameter1Soil1pH0238LY/T1239-1999Determination of pH value in forest soil2OrganicMatter0238LY/T 1237-1999Determination of organic matter in forest soil and calculation carbon-nitrogen rat

19、io3Water Content0238LY/T1213-1999Determination of forest soil water content1Soil4Total Nitrogen0238NY/T 53-1987Method for the determination of soil total nitrogen(Semi-micro Kjeldahl method)5TotalPhosphorus0238LY/T1232-1999Determination of total phosphorus in forest soil6AvailablePhosphorus0238LY/T1

20、233-1999Determination of available phosphorus in forest soil7TotalPotassium0238LY/T1234-1999Determination of total potassium in forest soil8AvailablePotassium0238LY/T1236-1999Determination of available potassium in forest soil9Water soluble salts of soil0238LY/T 1251-1999Analysis methods of water so

21、luble salts of forest soil10AvailableCopper0238LY/T 1260-1999Determination of available copper in forest soil11AvailableZinc0238LY/T 1261-1999Determination of available zinc in forest soil1Soil12AvailableIron0238LY/T 1262-1999Determination of available iron in forest soil13BHC, DDT0238GB/T 14550-200

22、3Method of gas chromatographic for determination of BHC and DDT in soil14C isotope-ratio analysis0238C isotope-radio mass spectrum analysis in organic compounds<Methods of agricultural chemistry analysis of soil > China Agricultural Science &Technology Press, 1999. p. 564-57015N isotope-ra

23、tio analysis0238N isotope radio mass spectrum analysis < Methods of agricultural chemistry analysis of soil > China Agricultural Science &Technology Press, 1999. p.558-5641Soil16TotalChromium0238HJ 4912009Soil quality Determination of total chromium Flame atomic absorption spectrometryExce

24、pt for 6.2.217Lead,Cadmium0238GB/T 171411997Soil quality-Determination of lead,cadmium-Graphite furnace atomic absorption spectrophotometry18Copper, Zinc0238GB/T 171381997Soil quality-Determination of copper, zinc-Flame atomic absorption spectrophotometry19Mercury0238GB/T 22105.1-2008Soil quality-An

25、alysis of total mercury, arsenic and lead contents-Atomic fluorescence spectrometry-Part1：Analysis of total mercury contents in soils1Soil20Total Arsenic0238GB/T 22105.2-2008Soil quality-analysis of total mercury, arsenic and lead contents-Atomic fluorescence spectrometry-Part2：Analysis of total ars

26、enic contents in soils21Conductivity0238DIN ISO 11265-1997Soil quality-Determination of the specific electrical conductivity22HydrolyzableNitrogen0238LY/T 1229-1999Determination of hydrolyzable nitrogen in forest soil23Ammonia,Nitrate,Nitrite Nitrogen0238ISO 14256-2-2005Soil quality-Determination of

27、 nitrate, nitrite, and ammonium in field-moist soils by extraction with potassium chloride solution-Part2: Automated method with segmented flow analysis1Soil24Chloride0238NY/T 1121.172006Soil Testing Part 17: Method for determination of soil chloride ion contentAccredited only for treatment methodHJ

28、/T 84-2001Water quality-Determination of inorganic anions-Ion chromatography methodAccredited only for determination method25Sulfate0238NY/T 1121.18-2006Soil Testing Part 18: Method for determination of soil sulfate contentHJ/T 84-2001Water quality-Determination of inorganic anions-Ion chromatograph

29、y method26Mineral Total Elements0238Lithium metaborate fusion-ICP-AES method <Methods of agricultural chemistry analysis of soil > China Agricultural Science &Technology Press, 1999. p. 45-571Soil27Total calcium,magnesium,sodium0238NY/T 296-1995Determination of total calcium, magnesium, so

30、dium in soil28Nickel0238GB/T17139-1997Soil quality-Determinationof nickel-Flame atomic absorption spectrophotometry29Total Selenium0238NY/T 1104-2006Determination of selenium in soils Atomic fluorescence spectrometry method30Organo-phosphorus pesticides0238GB/T 14552-2003Method of gas chromatographi

31、c for determination of organophosphorus pesticides in water and soil31Petroleum-hydrocarbon0238GB 17378.5-2007The specification for marine monitoring-Part 5: Sediment analysis2Air32N、O Isotopic composition to N2O in air0238GB/T 6041-2002 General rules for mass spectrometric analysis; Determination o

32、f nitrogen, carbon and oxygen stable isotope ratio in N2O, CH4 and CO2 at natural abundance levels by Mass Spectrometry，Acta pedologica sinca,Vol.45,No.2,Mar.,2008，pp249-25833C Isotopic composition to CH4 in air023834N Isotopic composition to N2 in air023835C、O Isotopic composition to CO2 in air0238

33、36CH4 content0238GB/T 8984-2008Determination of carbon monoxide, carbon dioxide and hydrocarbon in the gases-Gas chromatographic method2Air37CO2 content0238GB/T 18204.24-2000 Methods for determination of carbon dioxide in air of public place3Plant andFoods38BHC, DDT0227GB/T5009.19-2008Determination

34、of organochlorine pesticide multiresidues in foods39Ash0244GB/T5009.4-2010Determination of ash in foods40Total nitrogen,phosphorus,potassium0227LY/T 1269-1999 Determination of total nitrogen in forest plant and forest floor41Total phosphorus0227LY/T 1271-1999Determination of total nitrogen, phosphor

35、us, potassium, sodium, calcium, magnesium in forest plant and forest floor3Plant andFoods42Total potassium0227LY/T 1271-1999Determination of total nitrogen, phosphorus, potassium, sodium, calcium, magnesium in forest plant and forest floor43Cadmium0227GB/T5009.15-2003Determination of cadmium in food

36、sAccredited only for the first method44Total mercury0227GB/T 5009.17-2003Determination of total mercury and organic-mercury in foodsAccredited only for the first method45Lead0227GB/T5009.12-2010Determination of lead in foodsAccredited only for the first method46Selenium0227GB 5009.932010 National fo

37、od safety standard Determination of selenium in foodsAccredited only forthe first method3Plant andFoods47C isotope-ratio analysis0244C isotope-radio mass spectrum analysis in organic compounds<Methods of agricultural chemistry analysis of soil > China Agricultural Science &Technology Press

38、, 1999. p. 564-57048N isotope-ratio analysis0244N isotope radio mass spectrum analysis < Methods of agricultural chemistry analysis of soil > China Agricultural Science &Technology Press,1999 p. 558-56449pH0238GB/T6920-1986Water quality-Determination of pH value-Glass electrode method50Cop

39、per, Zinc, Lead,Cadmium0238GB/T 7475-1987Water quality-Determinationof copper, zinc, lead, cadmium-Atomic absorption spectrometry3Plant andFoods51Ammonium0238ISO 11732-2005 Water quality - Determination of ammonium nitrogen - Method by flow analysis (CFA and FIA) and spectrometric detection4Water52N

40、itrate0238ISO 13395-1996 Water quality - Determination of nitrite nitrogen and nitrate nitrogen and the sum of both by flow analysis (CFA and FIA) and spectrometric detection53Conductivity0238DZ/T0064.6-1993 Analysis method of ground water quality-Determination of electrical conductivity54Total salt

41、0238HJ/T 51-1999Water quality-Determination of total salt-Gravimetric method4Water55Total potassium0238EPA 200.7 Trace elements in water, solids, and biosolids by inductively coupled plasma-atomic emission spectrometry56Carbonate,Bicarbonate0238DZ/T0064.49-1993Analysis method of ground water quality

42、-Determination of carbonate, bicarbonate and hydroxyl-Titrimetric method57Chloride,Sulfate0238HJ/T 84-2001Water quality-Determination of inorganic anions-Ion chromatography method58Phosphate0238ISO 10304-1-2007Water quality-Determination of dissolved anions by liquid chromatography of ions-Part 1: D

43、etermination of bromide, chloride, fluoride, nitrate, nitrite phosphate and sulfate4Water59Aluminium0238EPA 200.7 Trace elements in water, solids, and biosolids by inductively coupled plasma-atomic emission spectrometry60Calcium,magnesium0238EPA 200.7 Trace elements in water, solids, and biosolids by inductively coupled plasma-atomic emission spectrometry61Iron,manganese0238EPA 200.7 Trace elements in water, solids, and biosolids by inductively coupled plasma-atomic emission spectrometry62Mercury0238SL 327.2-2005Water quality-determ