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干填料時(shí)△P/Z-u關(guān)系測(cè)定,,,,,,,,,,,,,,
L=0.80m填料層高度Z=0.75m塔徑D=0.05m,,,,,,,,,,,,,,
序號(hào),填料層壓降,單位高度填料層壓降,空氣轉(zhuǎn)子流量計(jì)讀數(shù),空塔氣速,,,,,不能刪,,,,,
,mmH2O,mmH2O/m,m3/h,m/s,,lgP/Z,lgu,,m3/s,,,,,
1,0.2,0.27,0.5,0.070737616,,-0.574031268,-1.150349578,,0.000138889,0.001963438,,,,
2,0.5,0.67,1.0,0.141475233,,-0.176091259,-0.849319582,,0.000277778,0.001963438,,,,
3,0.8,1.07,1.5,0.212212849,,0.028028724,-0.673228323,,0.000416667,0.001963438,,,,
4,0.9,1.20,2.0,0.282950466,,0.079181246,-0.548289586,,0.000555556,0.001963438,,,,
5,1.2,1.60,2.5,0.353688082,,0.204119983,-0.451379573,,0.000694444,0.001963438,,,,
,,,,,,,,,,0.001963438,,,,
濕填料時(shí)△P/Z-u關(guān)系測(cè)定,,,,,,,,,,0.001963438,,,,
L=0.80m填料層高度Z=0.75m塔徑D=0.05m,,,,,,,,,,0.001963438,,,,
序號(hào),填料層壓降,單位高度填料層壓降,空氣轉(zhuǎn)子流量計(jì)讀數(shù),空塔氣速,,,,,,0.001963438,,,,
,mmH2O,mmH2O/m,m3/h,m/s,,,,,,0.001963438,,,,
1,0.60,0.800000,0.5,0.070737616,,-0.096910013,-1.150349578,,0.000138889,0.001963438,,,,
2,1.00,1.333333333,0.7,0.099032663,,0.124938737,-1.004221542,,0.000194444,0.001963438,,,,
3,1.75,2.333333333,0.9,0.12732771,,0.367976785,-0.895077073,,0.00025,0.001963438,,,,
4,2.15,2.866666667,1.1,0.155622756,,0.457377197,-0.807926897,,0.000305556,0.001963438,,,,
5,2.90,3.866666667,1.3,0.183917803,,0.587336735,-0.73537623,,0.000361111,0.001963438,,,,
6,3.80,5.066666667,1.5,0.212212849,,0.704722333,-0.673228323,,0.000416667,0.001963438,,,,
7,5.30,7.066666667,1.7,0.240507896,,0.849214606,-0.618870661,,0.000472222,0.001963438,,,,
8,7.00,9.333333333,2.0,0.282950466,,0.970036777,-0.548289586,,0.000555556,0.001963438,,,,
9,10.00,13.33333333,2.3,0.325393036,,1.124938737,-0.487591746,,0.000638889,0.001963438,,,,
,,,,,,,,,,,,,填料吸收塔傳質(zhì)實(shí)驗(yàn)技術(shù)數(shù)據(jù)表,
,,,,,,,,,,,,,塔類型,吸收塔
,,,,,,,,,,,,,填料種類,瓷拉西環(huán)
,,,,,,,,,,,,,填料尺寸mm,φ6×10mm
,,,,,,,,,,,,,填料層高度m,0.76
,,,,,,,,,,,,,CO2轉(zhuǎn)子流量計(jì)讀數(shù)m3/h,0.1
,,,,,,,,,,,,,CO2轉(zhuǎn)子流量計(jì)處氨溫度℃,34.4
,,,,,,,,,,,,,流量計(jì)處CO2的體積流量m3/h,0.1
,,,,,,,,,,,,,水轉(zhuǎn)子流量計(jì)讀數(shù)L/h,0.2
,,,,,,,,,,,,,水流量L/h,0.2
,,,,,,,,,,,,,中和CO2用Ba(OH)2的濃度mol/L,0.1
,,,,,,,,,,,,,中和CO2用Ba(OH)2的體積mL,10.00
,,,,,,,,,,,,,滴定用鹽酸濃度mol/L,0.1
,,,,,,,,,,,,,滴定塔底吸收液用鹽酸體積mL,10.96
萃取實(shí)驗(yàn)基礎(chǔ)數(shù)據(jù)列表,,,,,,,1.64*10^3,,,,,,滴定空白液用鹽酸體積mL,11.80
塔型:槳葉式旋轉(zhuǎn)萃取塔塔內(nèi)徑:37mm溶質(zhì)A:苯甲酸,,,,,,,,,,,,,,
稀釋劑B:煤油萃取劑S:水連續(xù)相:水塔內(nèi)溫度:20℃,,,,,,,,,,,,,樣品體積mL,10
分散相:煤油煤油密度:800kg/m3塔有效高度:0.75m,,,,,,,,,,,,,塔底液相的溫度℃,16.3
項(xiàng)目/實(shí)驗(yàn)序號(hào),,,1,2,,,c1-c2,-0.0084,,,,,亨利系數(shù)E×105Pa,0.00166
槳葉轉(zhuǎn)速轉(zhuǎn)/分,,,90,90,,,H,3.38753E-05,,,,,塔底液相濃度c1kmol/m3,0.1096
水轉(zhuǎn)子流量計(jì)數(shù)L/h,,,4,4,,,,0.376100271,,,,,空白液相濃度c2kmol/m3,0.118
煤油轉(zhuǎn)子流量計(jì)數(shù)L/h,,,6,6,,,,,,,,,傳質(zhì)單元高度HL×10-7kmol/(m3Pa),2.34176653*108
"濃度
分析",NaOH溶液濃度mol/L,,0.01,0.01,,,ln,-0.032027104,,,,,平衡濃度c*10-2kmol/m3,37.61
,塔底輕相XRb,樣品體積ml,10,10,,,,,,,,,平均推動(dòng)力△cmkmolCO2/m2,0.26228
,,NaOH用量ml,0.2,0.22,,,dc2,0.258100271,,,,,液相體積傳質(zhì)系數(shù)KLam/s,17.39920
,塔頂輕相XR,樣品體積ml,10,10,,,dc1,0.266500271,,,,,,
,,NaOH用量ml,0.2,0.21,,,,,,,,,,
,塔底重相YBb,樣品體積ml,25,25,,,l/zo,543.2648947,,,,,,
,,NaOH用量ml,0.86,0.85,,,,,,,,,,
"計(jì)
算
及
實(shí)
驗(yàn)
結(jié)
果",塔底輕相濃度XRbkgA/kgB,,3.05×10-3,4.70×10-3,,,Hl,-23.41766539,0,0,,,,
,塔頂輕相濃度XRtkgA/kgB,,3.05×10-3,3.21×10-3,,,,0,,,,,,
,塔底重相濃度YBbkgA/kgB,,5.25×10-3,5.19×10-3,,,,0,0,,,,,
,水流量SkgS/h,,4,4,,,,,,,,,,
,煤油流量BkgB/h,,4.8,4.8,,,苯甲酸122,0.122kg,,,,,,
,傳質(zhì)單元數(shù)NOE(圖解積分),,3,3,,,煤油800,0.8,,,,,,
,傳質(zhì)單元高度HOE,,0.25,0.25,,,,,,,,,,
,體總傳質(zhì)系數(shù),KYeakgA/[m3?h?(kgA/kgs)],,17857.50202,17857.50202,,,面積,0.001075178,,,,,,
15℃,,,,,,,,,,,,,,
x,x*(y),x-x*,1/(x-x*),,,,,,,,,,,
0.01393,0.00275,0.01118,89.44543828,,,1.65,0.4125,,,,,,,
0.01252,0.002685,0.009835,101.6776817,,,,,,,,,,,
0.01201,0.002676,0.009334,107.1352046,,,2.0625,,,,,,,,
0.01275,0.002579,0.010171,98.31874939,,,,,,,,,,,
0.01082,0.002455,0.008365,119.5457262,,,,,,,,,,,
0.009721,0.002359,0.007362,135.8326542,,,,,,,,,,,
0.008276,0.002191,0.006085,164.3385374,,,,,,,,,,,
0.00722,0.002055,0.005165,193.6108422,,,,,,,,,,,
0.006384,0.00189,0.004494,222.5189141,,,,,,,,,,,
0.001897,0.001179,0.000718,1392.75766,,,,,,,,,,,
0.005279,0.001697,0.003582,27
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