江蘇珈誠紡織公司污泥鑒別項(xiàng)目初篩檢測(cè)報(bào)告rep19

1、Page 1 of 7檢測(cè)SHE19-00590：送交：聶鵬飛樣品采樣日期：2019/01/17大學(xué)環(huán)境規(guī)劃公2019/01/28客戶名稱：提交日期：司京市鼓樓區(qū)大學(xué)樣品：固體 (1)管理科學(xué)樓 14 樓項(xiàng)目：-備注：1.本公司，不得(全文除外) 檢測(cè)。2. 除非另有說明，僅對(duì)采樣及樣品測(cè)試負(fù)責(zé)。編制：審核：批準(zhǔn)：高級(jí)化學(xué)分析師Page 2 of 7VOC 檢索樣品VOCs 按USEPA Method 5035 進(jìn)行前處理,提取液根據(jù) US EPA Method 8260D 上GC/MS 儀分析,用NIST 譜庫定性檢索主要化合物，并以內(nèi)標(biāo) 1_4-Dichlorobenzene-d4(ISD

2、)為參考物進(jìn)行定 量，數(shù)據(jù)參考。19-00590-01客戶原標(biāo)識(shí)：板塊壓濾機(jī)1 0 0 0 0 08 0 0 0 06 0 0 0 04 0 0 0 02 0 0 0 07 .0 0T im e -序號(hào) R.T 面積%譜庫/ID參比#CAS#匹配度濃度1 12.170 10.472-乙基-1-己醇1.8 mg/kg1-Hexanol, 2-ethyl- 1-Hexanol, 2-ethyl-1-Hexanol, 2-ethyl-76-7 86-76-7 72-76-7 72Page 3 of 72 13.056 1.080.2 mg/kgMethyl 4-hydroxymandelatem,

3、2TMS d erivativeTetrasiloxane, 1,1,3,3,5,5,7,7-oct amethyl-9-Acridinol, trimethylsilyl ether203888 055334-40-2 63157181 001000-05-1 56140500 1000463-65-5 32QC-MB1 4 0 0 0 01 2 0 0 0 01 0 0 0 0 078 0 0 0 06 0 0 0 04 0 0 0 02 0 0 0 07 .0 0T im e -Page 4 of 7SVOC 檢索樣品 SVOCs 按USEPA Method 3570 進(jìn)行提取，根據(jù)US

4、EPA Method 8270E 用GC/MS 分析，NIST譜庫定性檢索主要化合物，并以內(nèi)標(biāo)Phenanthrene-D10 為參考物進(jìn)行半定量，數(shù)據(jù)參考。19-00590-01客戶原標(biāo)識(shí)：板塊壓濾機(jī)1200000110000010000009000008000007000009 . 7 2 1600000500000000003000002000001000001 0 . 0 0T i m e - - 序號(hào) R.T面積%譜庫/ID參比#CAS# 匹配度 濃度1 18.763 3.29十六烷9.0 mg/kgHexadecane HexadecaneHexadecane98285 00054

5、4-76-3 9598283 000544-76-3 9598286 000544-76-3 952 19.410 3.557-甲基十六烷9.7 mg/kgHexadecane, 7-methyl- TritetracontaneCarbonic acid, eicosyl vinyl ester112538 026730-20-1 80303428 007098-21-7 80243879 1000382-54-3 80Page 5 of 73 19.633 1.31 2-甲基十六烷3.6 mg/kgHexadecane, 2-methyl- Z-8-HexadeceneOcetracont

6、ane, 1-iodo-112540 001560-92-5 8396037 1000130-87-5 74306215 040710-70-1 704 20.121 5.64十七烷15.4 mg/kgHeptadecaneHeptadecane Pentadecane112529 000629-78-7 97112530 000629-78-7 9583511 000629-62-9 935 21.3544.73十八烷13.0 mg/kgOctadecane OctadecaneHexacosane127050 000593-45-3 98127049 000593-45-3 9124222

7、7 000630-01-3 906 21.431 4.342,6,10,14-四甲基十六烷11.9 mg/kgHexadecane, 2,6,10,14-tetramethyl-157097 000638-36-8 9898313 1000432-25-9 89302147 062108-51-4 833-Ethyl-2,6,10-trimethydecanePenriacontane, 1-bromo-7 22.494 4.2911.7 mg/kg十九烷NonadecaneNonadecane Nonadecane141973 000629-92-5 96141972 000629-92-5

8、 93141975 000629-92-5 938 23.5583.88二十烷10.6 mg/kgEicosaneCarbonic acid, eicosyl vinyl ester Carbonic acid, octadecyl vinyl est er157074 000112-95-8 95243879 1000382-54-3 90219338 1000382-54-4 90Page 6 of 74.9 mg/kg9 27.647 1.771,3,5-三苯基環(huán)己烷Cyclohexane, 1,3,5-triphenyl-9-Octadecenoic acid (Z)-, phenyl

9、me thyl esterCarbonic acid, ethyl pentadecyl ester190241 028336-57-4 92247467 055130-16-0 25176965 1000314-59-5 251028.041 4.3211.8 mg/kgCarbonic acid, 2-ethylhexyl octyl ester Carbonic acid, 2-ethylhexyl octadecyl esterCarbonic acid, 2-ethylhexyl tetradecyl ester161554 1000383-13-5 59277412 1000383

10、-14-5 58245742 1000383-14-1 541129.416 5.3014.5 mg/kgCarbonic acid, 2-ethylhexyl tetradecyl ester6-Octadecenoic acid2- Chloropropionic acid, hexadecyl ester245742 1000383-14-1 74156905 1000336-66-8 73211027 086711-81-1 721229.621 3.9610.8 mg/kgCarbonic acid, decyl 2-ethylhexyl ester Carbonic acid, 2-ethylhexyl octadecyl esterCarbonic acid, 2-ethylhexyl heptad192215 1000383-13-7 69277412 1000383-14-5 68271388 1000383-14-4 68Page 7 of 7ecyl esterQC-MB100000095000098050000000080000077500000000065000065050000