溶出儀操作與使用維護(hù)

操作，打開加熱泵開關(guān)、溶出儀開關(guān):開機(jī)后出現(xiàn)如下界面PleaseLogIn[SelectProtocol]PleaseLogInRPMSETPOINT:0RPMSETPOINT:0RPMELAPSEDTIME100.00:00100.00:0000TEMPSETPOINT:0.00年25.590:0025.590:0000RPMSETPIONT為設(shè)定的轉(zhuǎn)速、ELAPSEDTIME為已經(jīng)運(yùn)行的時間、TEMPSETONT溫度設(shè)定點(diǎn)、NEXTSAMPLE下次取樣時間。點(diǎn)擊篁￥覆鍵進(jìn)入功能菜單界面；1.3點(diǎn)擊protocols（方法1.3點(diǎn)擊protocols（方法）鍵進(jìn)入方法菜單界面;選擇運(yùn)行方法后退回主界面，如沒有編輯好的方法則創(chuàng)建方法。1.4創(chuàng)建方法：在10.1.7界面下點(diǎn)擊ADD鍵添加方法，進(jìn)入如下界面Labels1DissolutionSamplingProtocolNameMyProtocolMameMediaTypeWaterDrugNameMyDrugNameMediaVolume900MLDosage500mgOptions1ProtocolID00Q0-00D1Events|Apparatus 二CommentsHansonVISIONAutoPlus反［b11型］|?UFEXPORTVICOTVI|IDELETE|PRINT【EXH|A.點(diǎn)擊lebals(標(biāo)簽)鍵，在此項(xiàng)下輸入(protocolname)方法名稱、(drugname)產(chǎn)品名稱、(dosage)規(guī)格、(prttocolID)方法編號、(mediatype)溶媒介質(zhì)、(mediavolume)媒介體積；B.點(diǎn)擊dissolution溶出)鍵，在此項(xiàng)下輸入(drivespeed)轉(zhuǎn)速、(bathtemperature)水浴溫度、(testlength)運(yùn)行時間、其他項(xiàng)目默認(rèn)設(shè)置；DriveSpeed100RPMSpeedTolerance .巡.一Dissolution一iSamphng|BathTemperature3.7.00%"TemperatureTolerance0.50%TestLength2:00DigitalTempProbesEnabledOptionsIPrintInterval0:30VesselGoalTemperature36.95℃Events?、［dETI［篇1(￡］C.點(diǎn)擊sampling鍵，在此項(xiàng)下輸入(samplingmode)取樣方式、其他項(xiàng)目默認(rèn)設(shè)置;L曲豳|(zhì):SamplingMode:ManualMagazineTravel60mm,IDissolution:StaggerExtension:8minAul。DosageDeliveryDelay3￡位hamplinqOptionsEvents叼 B 1e昌|| x1EXPORT|I COPY V IDELETE |［PRUfTII EXIT|D.點(diǎn)擊options鍵，在此項(xiàng)下輸入(pre-startrinsetime)潤洗時間、(retrievalvolume)回補(bǔ)液體積、其他項(xiàng)目默認(rèn)設(shè)置；

Label??Auts-StartTestPromptInfinityTestLengthDisabledDissolution?Pre-StartRinseTime□secInunityTestSpeed ；□RPMSampling?BackflushFilterNoRetrievalVolume0.0mlOptionsAutoWashAtEndDisabledEventsEXPORTIcowDELETE◎Ur1PRINT1tEXIT1二一 L 、 E.點(diǎn)擊Events鍵，設(shè)置取樣點(diǎn)及取樣時間，設(shè)置完成后按EXIT鍵退出。Labels?PRE-RUNRinseVolume=4.004:DDSampleDissolution?一?Sarnphnq1:00:Sample5:002:00Sample6:閡SampleOptions?3:00:Sample7:00SampleEvents3:00DriveSpeed=100POST-RUN ；Print.StatisticsI星1ADOEVENT昌1PRINT1運(yùn)行：選擇方法后退回至主界面，待溫度達(dá)到設(shè)定溫度后^tart鍵運(yùn)行。準(zhǔn)備好取樣針，等待取樣，當(dāng)?shù)竭_(dá)取樣時間后進(jìn)行取樣。結(jié)束：實(shí)驗(yàn)完成后關(guān)閉電源，清洗取樣針和溶出杯。自動取樣操作：打開溶出儀電源、加熱泵電源和自動取樣器電源開關(guān)。打開自動取樣器后會出現(xiàn)如下界面：ELAPSEDTIME表示以經(jīng)運(yùn)行的時間，NEXTSAMPLE表示下次取樣時間，0.0ml處顯示取樣體積。點(diǎn)擊電期菜單鍵進(jìn)入功能菜單界面:點(diǎn)擊Protocols鍵進(jìn)入方法菜單界面:1AluminumEdfatez.fliTiDKcilincapsules3;AsprinCapsi.lea330mg4:EiarumSulfate5EenzylBenzcfate選擇需要的方法然后退回主界面，如沒有方法則創(chuàng)建方法。2.5創(chuàng)建方法：在2.4界面點(diǎn)擊ADD鍵添加方法，進(jìn)入如下界面:LabelsProtocolNameMediaTypeWaterDissolution?:DrugNamejMyDrugNameMediaVolume900ML5「ISamplingjDosage:500mgOptionsj:ProtocolID0000-0001Events?|ApparatusCommentsHansonVISIONAutoPlus叼r?irFir?iix]EXPORT*ICOPVl|IDELETE.(PRINT|IEXE1!A.點(diǎn)擊lebals(標(biāo)簽)鍵，在此項(xiàng)下輸入(protocolname)方法名稱、(drugname)產(chǎn)品名稱、(dosage)規(guī)格、(prttocolID)方法編號、(mediatype)溶媒介質(zhì)、(mediavolume)媒介體積；B.點(diǎn)擊dissolution溶出)鍵，在此項(xiàng)下輸入(drivespeed)轉(zhuǎn)速、(bathtemperature)水浴溫度、(testlength)運(yùn)行時間、其他項(xiàng)目默認(rèn)設(shè)置；

LabelsDriveSpeed100RPMSpeedTolerance4%DissolutionBathTemperature37.00℃TemperatureTolerance0.50℃SamplingTest2:00LengthDigitalTempProbesEnabledOptionsPrint0:30IntervalVesselGoalTemperature36.95℃C.點(diǎn)擊sampling鍵，在此項(xiàng)下輸入(SamplingMode)取樣方式、(RackType)取樣架型號、(RinseVolume)潤洗體積、(CollectVolumeLabelsDriveSpeed100RPMSpeedTolerance4%DissolutionBathTemperature37.00℃TemperatureTolerance0.50℃SamplingTest2:00LengthDigitalTempProbesEnabledOptionsPrint0:30IntervalVesselGoalTemperature36.95℃Labels|SamplingModeCollectAndDetectDetectVolume2.0mlDissolution|RackType16x100mmReadDelay5secSamplingRinseVolume7.0mlMagazineTravelLabels|SamplingModeCollectAndDetectDetectVolume2.0mlDissolution|RackType16x100mmReadDelay5secSamplingRinseVolume7.0mlMagazineTravel60mmOptionsjCollectVolume5.0mlAutuDosageDeliveryDelay3:secEventsMediaReplace12.0mlTesterOffsetTime0:05ru i-11k二1 hb、i曰「曩1「或1〔簿〕匚吸1E.點(diǎn)擊Events鍵，設(shè)置取樣點(diǎn)及取樣時間，設(shè)置完成后按EXIT鍵退出。LabelsPRE-RUNRinseVolume.=4.004:00 |SampleDissolution1:00Sample5:00SampleSampling2:00Sample6:00SampleOptions3:00Sample7:00SampleEvents13:00:DriveSpeed=100POST-RUNPrintStatistics2.6運(yùn)行：選擇方法后管置于試管架上。退回至主界面，待溫度達(dá)到設(shè)定溫度后2.6運(yùn)行：選擇方法后管置于試管架上。退回至主界面，待溫度達(dá)到設(shè)定溫度后年tart鍵運(yùn)行。準(zhǔn)備好試2.7結(jié)束：實(shí)驗(yàn)完成后清洗溶出儀管線和